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Super‐Reversible CuF<sub>2</sub> Cathodes Enabled by Cu<sup>2+</sup>‐Coordinated Alginate

Jiale Xia, Zeyi Wang, Nuwanthi D. Rodrig, Bo Nan, Jiaxun Zhang, Weiran Zhang, Brett L. Lucht, Chongyin Yang, Chunsheng Wang

2022Advanced Materials104 citationsDOIOpen Access PDF

Abstract

Abstract Copper fluoride (CuF 2 ) has the highest energy density among all metal fluoride cathodes owing to its high theoretical potential (3.55 V) and high capacity (528 mAh g −1 ). However, CuF 2 can only survive for less than five cycles, mainly due to serious Cu‐ion dissolution during charge/discharge cycles. Herein, copper dissolution is successfully suppressed by forming Cu 2+ ‐coordinated sodium alginate (Cu‐SA) on the surface of CuF 2 particles during the electrode fabrication process, by using water as a slurry solvent and sodium alginate (SA) as a binder. The trace dissolved Cu 2+ in water from CuF 2 can in situ cross‐link with SA binder forming a conformal Cu‐SA layer on CuF 2 surface. After water evaporation during the electrode dry process, the Cu‐SA layer is Li‐ion conductor but Cu 2+ insulator, which can effectively suppress the dissolution of Cu‐ions in the organic 4 m LiClO 4 /ethylene carbonate/propylene carbonate electrolyte, enhancing the reversibility of CuF 2 . CuF 2 electrode with SA binder delivers a reversible capacity of 420.4 mAh g ‐1 after 50 cycles at 0.05 C, reaching an energy density of 1009.1 Wh kg ‐1 . Cu 2+ cross‐link polymer coating on CuF 2 opens the door for stabilizing the high‐energy and low‐cost CuF 2 cathode for next‐generation Li‐ion batteries.

Topics & Concepts

Materials scienceDissolutionEthylene carbonateElectrolyteCathodeCopperChemical engineeringPropylene carbonateInorganic chemistryElectrodeMetallurgyChemistryEngineeringPhysical chemistryAdvancements in Battery MaterialsAdvanced Battery Materials and TechnologiesInorganic Fluorides and Related Compounds
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