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Highly Air‐Stable Single‐Crystalline β‐CsPbI<sub>3</sub> Nanorods: A Platform for Inverted Perovskite Solar Cells

Somnath Mahato, Arup Ghorai, S. K. Srivastava, M. Modak, Sudarshan Singh, S. K. Ray

2020Advanced Energy Materials73 citationsDOI

Abstract

Abstract The synthesis of single‐crystalline β‐CsPbI 3 perovskite nanorods (NRs) using a colloidal process is reported, exhibiting their improved photostability under 45–55% humidity. The crystal structure of CsPbI 3 NRs films is investigated using Rietveld refined X‐ray diffraction (XRD) patterns to determine crystallographic parameters and the phase transformation from orthorhombic (γ‐CsPbI 3 ) to tetragonal (β‐CsPbI 3 ) on annealing at 150 °C. Atomic resolution transmission electron microscopy images are utilized to determine the probable atomic distribution of Cs, Pb, and I atoms in a single β‐phase CsPbI 3 NR, in agreement with the XRD structure and selected area electron diffraction pattern, indicating the growth of single crystalline β‐CsPbI 3 NR. The calculation of the electronic band structure of tetragonal β‐CsPbI 3 using density functional theory (DFT) reveals a direct transition with a lower band gap and a higher absorption coefficient in the solar spectrum, as compared to its γ‐phase. An air‐stable (45–55% humidity) inverted perovskite solar cell, employing β‐CsPbI 3 NRs without any encapsulation, yields an efficiency of 7.3% with 78% enhancement over the γ‐phase, showing its potential for future low cost photovoltaic devices.

Topics & Concepts

Materials scienceTetragonal crystal systemOrthorhombic crystal systemNanorodPerovskite (structure)Band gapRietveld refinementSolar cellPerovskite solar cellCrystallographyCrystal structureDirect and indirect band gapsAnalytical Chemistry (journal)NanotechnologyOptoelectronicsChemistryChromatographyPerovskite Materials and ApplicationsQuantum Dots Synthesis And Properties2D Materials and Applications