Litcius/Paper detail

Multicomponent Assembly of Trisubstituted Imidazoles and Their Photochemical Cyclization into Fused Polyheterocyclic Scaffolds

Diana Gapanenok, Azat Makhmet, Anatoly A. Peshkov, Darya Smirnova, Niyaz Amire, Vsevolod A. Peshkov, Dar’ya V. Spiridonova, Dmitry Dar’in, Saeed Balalaie, Mikhail Krasavin

2022The Journal of Organic Chemistry12 citationsDOI

Abstract

A straightforward route to a large and diverse library of trisubstituted imidazoles was established via a three-component reaction of 2-oxoaldehydes, 1,3-dicarbonyl compounds, and acyclic nitrogen bis-nucleophiles. The obtained products were subsequently explored in a photochemical cyclization yielding a variety of imidazole-fused polycyclic compounds.

Topics & Concepts

ChemistryImidazoleNucleophileCombinatorial chemistryComponent (thermodynamics)Organic chemistryCatalysisThermodynamicsPhysicsMulticomponent Synthesis of HeterocyclesCatalytic C–H Functionalization MethodsChemical Synthesis and Analysis