Litcius/Paper detail

Evolution of the structure and dynamics of bovine serum albumin induced by thermal denaturation

Olga Matsarskaia, Lena Bühl, Christian Beck, Marco Grimaldo, Ralf Schweins, Fajun Zhang, Tilo Seydel, Frank Schreiber, Felix Roosen‐Runge

2020Physical Chemistry Chemical Physics42 citationsDOIOpen Access PDF

Abstract

O with and without NaCl. Using small-angle scattering, we provide information on structure before, during and after denaturation. Using quasi-elastic neutron scattering, we monitor in real-time the microscopic dynamics and dynamical confinement throughout the entire denaturation process covering protein unfolding and cross-linking. After denaturation, the protein dynamics is slowed down in salty solutions compared to those in pure water, while the stability and dynamics of the native solution appears unaffected by salt. The approach presented here opens opportunities to link microscopic dynamics to emerging structural properties, with implications for assembly processes in soft and biological matter.

Topics & Concepts

Denaturation (fissile materials)Bovine serum albuminChemistryNeutron scatteringChemical physicsSmall-angle neutron scatteringQuasielastic neutron scatteringCrystallographyThermalMolecular dynamicsDynamics (music)BiophysicsStructure factorScatteringThermodynamicsComputational chemistryChromatographyPhysicsOpticsBiologyNuclear chemistryAcousticsProtein Structure and DynamicsSpectroscopy and Quantum Chemical StudiesNMR spectroscopy and applications