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Nickel-catalyzed asymmetric reductive arylation of α-chlorosulfones with aryl halides

Deli Sun, Guobin Ma, Xinluo Zhao, Chuanhu Lei, Hegui Gong

2021Chemical Science43 citationsDOIOpen Access PDF

Abstract

We report an asymmetric Ni-catalyzed reductive cross-coupling of aryl/heteroaryl halides with racemic α-chlorosulfones to afford enantioenriched sulfones. The reaction tolerates a variety of functional groups under mild reaction conditions, which complements the current methods. The utility of this work was demonstrated by facile late-stage functionalization of commercial drugs.

Topics & Concepts

HalideArylNickelCatalysisReductive eliminationChemistryCombinatorial chemistryOrganic chemistryMedicinal chemistryAlkylSulfur-Based Synthesis TechniquesCatalytic C–H Functionalization MethodsRadical Photochemical Reactions
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