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Combined Use of Surface Texturing, Plasma Nitriding and DLC Coating on Tool Steel

Elisangela Aparecida dos Santos de Almeida, Júlio César Giubilei Milan, César Edil da Costa, Cristiano Binder, José Daniel Biasoli de Mello, Henara Lillian Costa

2021Coatings23 citationsDOIOpen Access PDF

Abstract

In cold rolling, a textured roll can be used to imprint a desired surface topography onto the sheet during rolling. This work proposes the use of diamond-like carbon (DLC) coatings to protect the surface topography of the rolls in replacement of the carcinogenic hard chrome. For that, hydrogenated amorphous carbon (a-C:H) was deposited on plasma nitrided tool steel, both for ground and textured specimens. Changes in surface topography due to DLC coating were assessed using a confocal microscope. Coating adhesion was evaluated using the method VDI 3198. The specimens were characterized using X-ray diffraction (XRD), microhardness test and scanning electron microscopy (SEM). The coating was characterized using Raman spectroscopy (RS) and X-ray photoelectron spectroscopy (XPS). The results showed a soft multilayer coating consisting of a plasma nitrided layer for load support, a Si-rich interlayer to improve adhesion and an a-C:H top layer. DLC deposition reduced the roughness of the textured specimens. The coating resulted in relatively stable friction and good durability, with small damage and negligible wear even under dry sliding.

Topics & Concepts

Materials scienceCoatingNitridingScanning electron microscopeX-ray photoelectron spectroscopyLayer (electronics)Diamond-like carbonSurface roughnessComposite materialRaman spectroscopyIndentation hardnessSurface finishAmorphous carbonMetallurgyThin filmMicrostructureChemical engineeringNanotechnologyOpticsPhysicsEngineeringDiamond and Carbon-based Materials ResearchMetal and Thin Film MechanicsLubricants and Their Additives
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