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Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber

Eliana Agaliotis, Baltazar D. Ake-Concha, A. May‐Pat, Juan P. Morales-Arias, Celina Bernal, Alex Valadez-González, P.J. Herrera‐Franco, Gwénaëlle Proust, J. Francisco Koh-Dzul, J.G. Carrillo, E.A. Flores‐Johnson

2022Polymers99 citationsDOIOpen Access PDF

Abstract

Natural fiber-reinforced composite (NFRC) filaments for 3D printing were fabricated using polylactic acid (PLA) reinforced with 1-5 wt% henequen flour comprising particles with sizes between 90-250 μm. The flour was obtained from natural henequen fibers. NFRCs and pristine PLA specimens were printed with a 0° raster angle for tension tests. The results showed that the NFRCs' measured density, porosity, and degree of crystallinity increased with flour content. The tensile tests showed that the NFRC Young's modulus was lower than that of the printed pristine PLA. For 1 wt% flour content, the NFRCs' maximum stress and strain to failure were higher than those of the printed PLA, which was attributed to the henequen fibers acting as reinforcement and delaying crack growth. However, for 2 wt% and higher flour contents, the NFRCs' maximum stress was lower than that of the printed PLA. Microscopic characterization after testing showed an increase in voids and defects, with the increase in flour content attributed to particle agglomeration. For 1 wt% flour content, the NFRCs were also printed with raster angles of ±45° and 90° for comparison; the highest tensile properties were obtained with a 0° raster angle. Finally, adding 3 wt% content of maleic anhydride to the NFRC with 1 wt% flour content slightly increased the maximum stress. The results presented herein warrant further research to fully understand the mechanical properties of printed NFRCs made of PLA reinforced with natural henequen fibers.

Topics & Concepts

Materials scienceComposite materialUltimate tensile strengthPolylactic acidCrystallinityWood flourNatural fiberFiberPolymerAdditive Manufacturing and 3D Printing Technologiesbiodegradable polymer synthesis and propertiesBone Tissue Engineering Materials
Tensile Behavior of 3D Printed Polylactic Acid (PLA) Based Composites Reinforced with Natural Fiber | Litcius