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Effect of current density on the microstructure and morphology of the electrodeposited nickel coatings

Amel Boukhouiete, Saliha Boumendjel, Nour-El-Houda SOBHI

2021TURKISH JOURNAL OF CHEMISTRY35 citationsDOIOpen Access PDF

Abstract

The aim of this research work was to study the effect of deposition current density on microstructure and surface morphology of electrodeposited nickel coatings. For this purpose, nickel deposits have been synthesized by direct current from Watts bath without additive, to limit the incorporation of pollutants resulting from surface adsorption or electro-activity of these compounds. Nickel deposits have been investigated by scanning electron microscopy and X-ray diffraction. Cyclic voltammetry was also used to gain information on the general behavior of the deposition. The optimum conditions of deposition were established and the influence of current density on the grain size, surface morphology, and crystal orientation was determined.

Topics & Concepts

NickelMicrostructureChemistryScanning electron microscopeCurrent densityCyclic voltammetryDeposition (geology)Morphology (biology)AdsorptionElectroplatingGrain sizeChemical engineeringMetallurgyDiffractionComposite materialElectrochemistryMaterials scienceElectrodeCrystallographyOrganic chemistryOpticsPhysical chemistryPaleontologyBiologyGeneticsQuantum mechanicsEngineeringLayer (electronics)SedimentPhysicsElectrodeposition and Electroless CoatingsCorrosion Behavior and Inhibition