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High-Spin ( <i>S</i> = 1) Blatter-Based Diradical with Robust Stability and Electrical Conductivity

Shuyang Zhang, Maren Pink, Tobias Junghoefer, Wenchao Zhao, Sheng‐Ning Hsu, Suchada Rajca, Arrigo Calzolari, Bryan W. Boudouris, Maria Benedetta Casu, Andrzej Rajca

2022Journal of the American Chemical Society76 citationsDOIOpen Access PDF

Abstract

is observed, favoring the triplet ground state over the singlet ground-state conformation in the 110-330 K temperature range. The diradical with the triplet ground-state conformation is found exclusively in crystals and in a polystyrene matrix. The crystalline neutral diradical is a good electrical conductor with conductivity comparable to the thoroughly optimized bis(thiazolyl)-related monoradicals. This is surprising because the triplet ground state implies that the underlying π-system is cross-conjugated and thus is not compatible with either good conductance or electron delocalization. The diradical is evaporated under ultra-high vacuum to form thin films, which are stable in air for at least 18 h, as demonstrated by X-ray photoelectron and electron paramagnetic resonance (EPR) spectroscopies.

Topics & Concepts

DiradicalChemistrySinglet stateGround stateElectron paramagnetic resonanceUnpaired electronTriplet stateMoleculeCrystallographyNuclear magnetic resonanceAtomic physicsOrganic chemistryExcited statePhysicsOrganic and Molecular Conductors ResearchMagnetism in coordination complexesElectron Spin Resonance Studies