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Comparative Analysis of Volatile Flavor Compounds in Seven Mustard Pastes via HS-SPME–GC–MS

Miao Liang, Rui Wang, Yajian Wu, Runhu Xin, Wei Guan, Yuping Liu

2023Molecules10 citationsDOIOpen Access PDF

Abstract

To identify the volatile flavor components in mustard paste (MP), the volatile compounds in seven MPs available on the market were isolated and analyzed by headspace solid-phase microextraction combined with gas chromatography-mass spectrometry. A total of 27 volatile constituents were found by mass spectra and retention index compared to the data obtained from reference compounds or the related literature and databases; these compounds included nine esters, three sulfur-containing compounds, two nitriles, three ketones, three alkenes, and seven other compounds. Of the 27 compounds, 6 compounds came from the turmeric added to MPs. Among the components detected, some compounds derived from AITC were allyl thiocyanate, carbon disulfide, allyl mercaptan, diallyl sulfide, and diallyl disulfide. The results obtained provide a better and comprehensive recognition of the volatile flavor compounds in MPs, and have some reference values for developing and applying isothiocyanate compounds.

Topics & Concepts

ChemistryDiallyl disulfideAllyl isothiocyanateDimethyl disulfideGas chromatography–mass spectrometryFlavorMass spectrometrySolid-phase microextractionCarbon disulfideChromatographyIsothiocyanateCarbonyl sulfideKovats retention indexDimethyl trisulfideSulfurGas chromatographyOrganosulfur compoundsOrganic chemistryFood scienceBiochemistryApoptosisPhytochemicals and Antioxidant ActivitiesEssential Oils and Antimicrobial ActivityFermentation and Sensory Analysis