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Surface Chemistry and Catalytic Reactivity of Borocarbonitride in Oxidative Dehydrogenation of Propane

Guangming Wang, Shunhua Chen, Qiwei Duan, Fenfei Wei, Sen Lin, Zailai Xie

2023Angewandte Chemie International Edition23 citationsDOIOpen Access PDF

Abstract

Abstract Borocarbonitride (BCN) materials are newly developed oxidative dehydrogenation catalysts that can efficiently convert alkanes to alkenes. However, BCN materials tend to form bulky B 2 O 3 due to over‐oxidation at the high reaction temperature, resulting in significant deactivation. Here, we report a series of super stable BCN nanosheets for the oxidative dehydrogenation of propane (ODHP) reaction. The catalytic performance of the BCN nanosheets can be easily regulated by changing the guanine dosage. The control experiment and structural characterization indicate that the introduction of a suitable amount of carbon could prevent the formation of excessive B 2 O 3 from BCN materials and maintain the 2D skeleton at a high temperature of 520 °C. The best‐performing catalyst BCN exhibits 81.9 % selectivity towards olefins with a stable propane conversion of 35.8 %, and the propene productivity reaches 16.2 mmol h −1 g −1 , which is much better than hexagonal BN (h‐BN) catalysts. Density functional theory calculation results show that the presence of dispersed rather than aggregated carbon atoms can significantly affect the electronic microenvironment of h‐BN, thereby boosting the catalytic activity of BCN.

Topics & Concepts

DehydrogenationPropaneCatalysisPropeneChemistrySelectivityReactivity (psychology)Density functional theoryPhotochemistryChemical engineeringOrganic chemistryComputational chemistryEngineeringPathologyMedicineAlternative medicineCatalysis and Oxidation ReactionsCatalytic Processes in Materials ScienceZeolite Catalysis and Synthesis