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Tailored Cathode Composite Microstructure Enables Long Cycle Life at Low Pressure for All-Solid-State Batteries

Ke Zhou, Sijian Lu, Charles Mish, Yu‐Ting Chen, Shijie Feng, Ji Young Kim, Min‐Sang Song, Hyunsun A. Kim, Ping Liu

2025ACS Energy Letters19 citationsDOI

Abstract

The practical application of all-solid-state batteries (ASSBs) requires reliable operation at low pressures, which remains a significant challenge. In this work, we examine the role of a cathode composite microstructure composed of solid-state electrolyte (SSE) with different particle sizes. A composite made of LiNi 0.8 Co 0.1 Mn 0.1 O 2 (NCM811) and fine-particle Li 6 PS 5 Cl (LPSC) shows a more uniform distribution of SSE on the surface of NCM811 particles, ensuring intimate contact. Moreover, the composite features reduced tortuosity, which enhances Li ion conduction. These microstructural advantages result in significantly reduced charge transfer resistance, helping to suppress mechanical distortion and electrochemical degradation during cycling under low-pressure conditions. As a result, the fine-LPSC cathode composite exhibits enhanced cycling stability at a moderate stack pressure of 2 MPa, outperforming its coarse-LPSC counterpart. Our finding confirms the important role of microstructure design in enabling high-performance ASSBs operating under low-pressure conditions.

Topics & Concepts

MicrostructureComposite numberMaterials scienceCathodeSolid-stateHigh pressureMetallurgyComposite materialEngineering physicsElectrical engineeringEngineeringAdvancements in Battery MaterialsAdvanced Battery Materials and TechnologiesAdvanced Battery Technologies Research