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Facile synthesis of sulfinate esters from aryl iodides <i>via</i> direct oxidation of thioesters

Keisuke Nakamura, Yukiko Kumagai, Akihiro Kobayashi, Minori Suzuki, Suguru Yoshida

2023Organic & Biomolecular Chemistry12 citationsDOIOpen Access PDF

Abstract

A practical method to synthesize sulfinate esters from aryl iodides is disclosed. Direct oxidation of thioesters prepared by copper-catalyzed C-S formation of aryl iodides realized the efficient synthesis of sulfinate esters. Due to the good accessibility of aryl iodides, a wide variety of sulfinate esters were prepared from easily available starting materials such as carboxylic acids and anilines.

Topics & Concepts

ChemistryArylOrganic chemistryCombinatorial chemistryCopperAlkylSulfur-Based Synthesis TechniquesChemical Synthesis and ReactionsCatalytic C–H Functionalization Methods
Facile synthesis of sulfinate esters from aryl iodides <i>via</i> direct oxidation of thioesters | Litcius