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Lithium Pyrene Squarate Covalent Organic Frameworks for Efficient Lithium and Magnesium Separation from Salt Water

Ataf Ali Altaf, Ahmadreza Khosropour, Amin Zadehnazari, Alireza Abbaspourrad

2023ACS Applied Materials & Interfaces16 citationsDOI

Abstract

The increasing pressure for lithium resources from the electric vehicle and nuclear energy industries means that new technologies to separate Mg 2+ from Li + from salt water are in demand. To address this need, we fabricated lithium pyrene squarate covalent organic frameworks (Li-SQCOFs) to separate Mg 2+ /Li + mixtures from salt water. We optimized the effect of the electrolyte and the amount of the adsorbent and then carried out a kinetics study on the adsorbent recovery at various pH levels using both batch and continuous flow adsorption methods. Li-SQCOF was found to have excellent selectivity for solutions containing a mixture of Mg 2+ /Li + ions. This work represents a unique path for the separation of Mg 2+ /Li + through direct adsorption using a covalent organic framework (COF). The COF-supported ultrafiltration bed made in this study gave a Mg 2+ separation flux of 60.5 h –1 m –2 .

Topics & Concepts

Lithium (medication)AdsorptionCovalent organic frameworkSalt (chemistry)Covalent bondMaterials scienceElectrolytePyreneInorganic chemistrySelectivityIon exchangeChemical engineeringIonChemistryElectrodeOrganic chemistryCatalysisEngineeringMedicinePhysical chemistryEndocrinologyExtraction and Separation ProcessesCovalent Organic Framework ApplicationsChemical Synthesis and Characterization
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