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Ni-Catalyzed Synthesis of Thiocarboxylic Acid Derivatives

John J. Monteith, Katerina Scotchburn, L. Reginald Mills, Sophie A. L. Rousseaux

2022Organic Letters16 citationsDOI

Abstract

-alkyl xanthate esters or thiocarbonyl imidazolides and organozinc reagents for the synthesis of thiocarboxylic acid derivatives has been developed. This method benefits from a fast reaction time, mild reaction conditions, and ease of starting material synthesis. The use of transition-metal catalysis to access a diverse range of thiocarbonyl-containing compounds provides a useful complementary approach when compared with previously established methodologies.

Topics & Concepts

ChemistryXanthateCatalysisReagentAlkylOrganic chemistryTransition metalCombinatorial chemistryReaction conditionsSulfur-Based Synthesis TechniquesCyclopropane Reaction MechanismsSynthesis and Catalytic Reactions
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