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Magnetically Induced CO <sub>2</sub> Methanation Using Exchange‐Coupled Spinel Ferrites in Cuboctahedron‐Shaped Nanocrystals

B. Rivas‐Murias, Juan M. Asensio, Nicolas Mille, Benito Rodríguez‐González, Pier‐Francesco Fazzini, J. Carrey, Bruno Chaudret, Verónica Salgueiriño

2020Angewandte Chemie International Edition32 citationsDOIOpen Access PDF

Abstract

Abstract Magnetically induced catalysis can be promoted taking advantage of optimal heating properties from the magnetic nanoparticles to be employed. However, when unprotected, these heating agents that are usually air‐sensitive, get sintered under the harsh catalytic conditions. In this context, we present, to the best of our knowledge, the first example of air‐stable magnetic nanoparticles that: 1) show excellent performance as heating agents in the CO 2 methanation catalyzed by Ni/SiRAlOx, with CH 4 yields above 95 %, and 2) do not sinter under reaction conditions. To attain both characteristics we demonstrate, first the exchange‐coupled magnetic approach as an alternative and effective way to tune the magnetic response and heating efficiency, and second, the chemical stability of cuboctahedron‐shaped core–shell hard CoFe 2 O 4 –soft Fe 3 O 4 nanoparticles.

Topics & Concepts

SpinelNanocrystalMaterials scienceMethanationChemical engineeringChemistryNanotechnologyMetallurgyCatalysisEngineeringBiochemistryMagnetic Properties and Synthesis of FerritesMagnetic Properties of AlloysMetallic Glasses and Amorphous Alloys
Magnetically Induced CO <sub>2</sub> Methanation Using Exchange‐Coupled Spinel Ferrites in Cuboctahedron‐Shaped Nanocrystals | Litcius