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Photocatalytic three-component annulation enabling stereoselective generation of (<i>Z</i>)-thiochromene 1,1-dioxides

Kexian Song, Xiao‐Yan Qin, Zixuan Ma, Fang-Zhou Geng, Wen‐Juan Hao, Shu‐Jiang Tu, Bo Jiang

2021Organic Chemistry Frontiers30 citationsDOI

Abstract

A new photocatalytic three-component annulation of 2-alkynylaryldiazonium tetrafluoroborates with γ-hydroxyl terminal alkynes and sodium metabisulfite is reported and used to produce a series of ( Z )-thiochromene 1,1-dioxides.

Topics & Concepts

AnnulationChemistryStereoselectivityPhotocatalysisComponent (thermodynamics)Sodium metabisulfiteOrganic chemistryCombinatorial chemistryMedicinal chemistryCatalysisPhysicsThermodynamicsSulfur-Based Synthesis TechniquesRadical Photochemical ReactionsOxidative Organic Chemistry Reactions