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Concentrating Nitrogen Waste with Electrodialysis for Fertilizer Production

Mohammed Tahmid, Hyuck Joo Choi, Sai Tarun Ganapavarapu, Joseph K. Scott, Marta C. Hatzell

2024Environmental Science & Technology Letters18 citationsDOIOpen Access PDF

Abstract

High Resolution Image Download MS PowerPoint Slide Recovery of nitrogen from wastewater presents a unique opportunity to valorize waste and contribute to a more circular nitrogen economy. However, dilute solution separations are challenging for most state-of-the-art separations technologies. This often results in technologies having low concentration factors that result in low-value products (e.g., < 1 wt % N). Here, we demonstrate how a cascading electrodialysis system combined with a hollow fiber membrane contactor (ED+HFMC) system can achieve efficient recovery of ammonia from simulated centralized animal feeding operation (CAFO) wastewater. The integrated system achieved an overall concentration factor of ∼200× (∼40× in ED and ∼5× in HFMC). This resulted in a ∼10 wt % NH 4 + -N fertilizer product. The specific energy consumption (SEC) for the three stages of the ED was 1.89–6.14 kWh/kg NH 4 + -N, which is lower than that of the Haber–Bosch process (8.9–19.3 kWh/kg N). Operating costs were <$0.90/kg NH 4 + -N for each of the electrodialysis stages and NH 3 stripping. This integrated ED+HFMC system holds promise for the recovery of ammonia from dilute feedstreams as the ED+HFMC achieves high concentration factors and has low energy demand.

Topics & Concepts

ElectrodialysisProduction (economics)FertilizerEnvironmental scienceWaste managementChemistryEngineeringMembraneEconomicsOrganic chemistryMacroeconomicsBiochemistryMembrane-based Ion Separation TechniquesAmmonia Synthesis and Nitrogen ReductionMembrane Separation Technologies
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