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Synthesis of Novel Hybrid Heterocycles Tethered 2,3‐Diphenoxyquinoxaline Moiety via Hantzsch, Michael, and Biginelli Reactions: Antimicrobial Activities and Molecular Docking Simulation

Hadeer M. Diab, Doaa Hassan Ali, Tayseer A. Abdallah, Mona M. Soliman, Ahmed H. M. Elwahy, Ismail A. Abdelhamid, Mostafa E. Salem, Ibrahim M. Z. Fares

2025Journal of Heterocyclic Chemistry10 citationsDOI

Abstract

ABSTRACT In this study, we have developed new hybrid compounds by connecting bis‐heterocycles with a 2,3‐diphenoxyquinoxaline core. This is performed by combining 4,4′‐(quinoxaline‐2,3‐diylbis(oxy))dibenzaldehyde with the necessary reagents via Hantzsch and Biginelli reactions. The newly synthesized compounds' structures are determined by elemental analysis, 1 H NMR, 13 C NMR, IR, and MS spectra. The tested compound 18 has the strongest antibacterial activities against S. aureus and E. coli , with inhibition zones of 18 and 14.67 mm, respectively. The tested compound 5 exhibited the strongest antibacterial activities against S. aureus , with an inhibition zone of 17 mm. Molecular docking studies of the most efficient compounds were performed against two proteins, including ATP‐dependent Clp protease ATP‐binding subunit ClpA (UniProt ID: P0ABH9) and Glycerol dehydrogenase (GDH) (UniProt ID: P0A9S5). Compound 5 interacted with the ClpA active site, exhibiting a binding score of ∆G = −9.2 Kcal/mol, while 18 interacted with the GDH active site, exhibiting a binding score of ∆G = −11.4 Kcal/mol.

Topics & Concepts

ChemistryMoietyCombinatorial chemistryDocking (animal)Active siteAntimicrobialStereochemistryReagentProtein subunitProteaseMolecular modelAntibacterial activityAntifungalEnzymeOrganic chemistryChemical synthesisBinding siteGlycerolMonomerBiginelli reactionSynthesis and Biological EvaluationSynthesis and biological activitySynthesis and Characterization of Heterocyclic Compounds