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Synthesis and crystal structure of 1-((3<i>R</i>,10<i>S</i>,13<i>R</i>,17<i>S</i>)-10,13-dimethyl-3-(<i>p</i>-tolylamino)hexadecahydro-1<i>H</i>-cyclopenta-[a]phenanthren-17-yl)ethan-1-one, C<sub>28</sub>H<sub>41</sub>NO

Hua Huang, Wen-Wen Zhang, Jiang-Hai Ye, Juan Zou, Kang He

2022Zeitschrift für Kristallographie - New Crystal Structures10 citationsDOIOpen Access PDF

Abstract

Abstract C 28 H 41 NO, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.5758(10) Å, b = 12.3659(9) Å, c = 18.0301(16) Å, V = 2358.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0524, wR ref ( F 2 ) = 0.1220, T = 273(2) K.

Topics & Concepts

Orthorhombic crystal systemCrystallographyCrystal structureChemistryPhysicsStereochemistryMicrobial Natural Products and BiosynthesisRadical Photochemical ReactionsAxial and Atropisomeric Chirality Synthesis
Synthesis and crystal structure of 1-((3<i>R</i>,10<i>S</i>,13<i>R</i>,17<i>S</i>)-10,13-dimethyl-3-(<i>p</i>-tolylamino)hexadecahydro-1<i>H</i>-cyclopenta-[a]phenanthren-17-yl)ethan-1-one, C<sub>28</sub>H<sub>41</sub>NO | Litcius