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Magnetic field-assisted solidification of W319 Al alloy qualified by high-speed synchrotron tomography

Zihan Song, Élodie Boller, Alexander Rack, Peter Lee, Biao Cai

2022Journal of Alloys and Compounds13 citationsDOIOpen Access PDF

Abstract

Magnetic fields have been widely used to control solidification processes. Here, high-speed synchrotron X-ray tomography was used to study the effect of magnetic fields on solidification. We investigated vertically upward directional solidification of an Al-Si-Cu based W319 alloy without and with a transverse magnetic field of 0.5 T while the sample was rotating. The results revealed the strong effect of a magnetic field on both the primary α-Al phase and secondary β-Al5FeSi intermetallic compounds (IMCs). Without the magnetic field, coarse primary α-Al dendrites were observed with a large macro-segregation zone. When a magnetic field is imposed, much finer dendrites with smaller primary arm spacing were obtained, while macro-segregation was almost eliminated. Segregated solutes were pushed out of the fine dendrites and piled up slightly above the solid/liquid interface, leading to a gradient distribution of the secondary β-IMCs. This work demonstrates that rotating the sample under a transversal magnetic field is a simple yet effective method to homogenise the temperature and composition distributions, which can be used to control the primary phase and the distribution of iron-rich intermetallics during solidification.

Topics & Concepts

SynchrotronIntermetallicAlloyMagnetic fieldMaterials scienceDirectional solidificationPhase (matter)Rotating magnetic fieldMicrostructureMetallurgyMagnetCondensed matter physicsOpticsChemistryPhysicsQuantum mechanicsOrganic chemistryAluminum Alloy Microstructure PropertiesSolidification and crystal growth phenomenaMetallurgical Processes and Thermodynamics
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