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SO<sub>2</sub>-Poisoning-Resistant CeO<sub>2</sub>@TiO<sub>2</sub> Nanorod with the core–shell Structure for the Catalytic Oxidation of CO

Qi Gao, Changqing Dong, Xiaoying Hu, Junjiao Zhang, Quanjun Zheng, Junjie Xue, Ying Zhao, Xiao Wang

2023The Journal of Physical Chemistry C10 citationsDOI

Abstract

The core–shell-structured CeO 2 @TiO 2 nanorods and traditional CeTiO x nanoparticles were prepared to study the role of the core–shell structure in CO catalytic oxidation and SO 2 resistance. CeO 2 @TiO 2 maintained a higher than 98% CO conversion at 300 °C in the flue gas containing 1000 ppm CO and achieved about 68% CO conversion after adding 500 ppm SO 2 for 5 h. The core–shell structure mitigated the crystallinity loss of the CeO 2 core and pore blockage of CeO 2 @TiO 2 . TiO 2 avoided the reaction between SO 2 and CeO 2 to protect CeO 2 from SO 2 poisoning. In the case of SO 2 passing through the shell, TiO 2 could inhibit the formation of Ce 2 (SO 4 ) 3, delaying the deactivation of the CeO 2 core. Furthermore, the sulfate deposited on CeO 2 @TiO 2 possessed a smaller amount and poorer thermal stability than that on CeTiO x . The design of the core–shell structure provides an effective route to enhance the SO 2 -poisoning resistance of catalysts in CO oxidation.

Topics & Concepts

NanorodCatalysisMaterials scienceShell (structure)CrystallinityChemical engineeringFlue gasThermal stabilitySulfateNanotechnologyChemistryComposite materialMetallurgyOrganic chemistryEngineeringCatalytic Processes in Materials ScienceCatalysis and Oxidation ReactionsIndustrial Gas Emission Control
SO<sub>2</sub>-Poisoning-Resistant CeO<sub>2</sub>@TiO<sub>2</sub> Nanorod with the core–shell Structure for the Catalytic Oxidation of CO | Litcius