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Synthesis, Characterization, and Catalytic Application of SnP <sub>2</sub> O <sub>7</sub> for the Highly Efficient Synthesis of Xanthene Derivatives

Youssef Merroun, Soukaina Chehab, Achraf El Hallaoui, Taoufiq Guedira, Saı̈d Boukhris, Rachida Ghaılane, Abdelaziz Souızı

2023Polycyclic aromatic compounds16 citationsDOI

Abstract

This study introduces a mono-ammonium phosphate-based heterogeneous catalyst that possesses characteristics of simplicity, reusability, and recoverability, making it well-suited for multicomponent reactions. The prepared catalyst underwent comprehensive characterization using Fourier-transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) patterns, scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX). Employing this catalyst in a one-pot multicomponent approach, it becomes possible to synthesize xanthene derivatives efficiently. The results showcase the impressive performance of the novel SnP2O7, which acts as a heterogeneous catalyst in traditional reactions, leading to the desired products with yields ranging from good to excellent and within a short reaction time. Notably, SnP2O7 exhibits remarkable stability in its catalytic activity, enabling its use for up to five cycles without experiencing a significant decrease in yield.

Topics & Concepts

XantheneCatalysisChemistryReusabilityCharacterization (materials science)Fourier transform infrared spectroscopyYield (engineering)Scanning electron microscopeSpectroscopyHeterogeneous catalysisCombinatorial chemistryChemical engineeringNanotechnologyOrganic chemistryMaterials scienceComputer scienceProgramming languagePhysicsQuantum mechanicsComposite materialMetallurgyEngineeringSoftwareMulticomponent Synthesis of HeterocyclesSynthesis of Organic CompoundsChemical Synthesis and Reactions