Litcius/Paper detail

Extracting information from X-ray diffraction patterns containing Laue oscillations

Aaron Miller, Mellie Lemon, Marisa A. Choffel, Sarah R. Rich, Fischer Harvel, David C. Johnson

2022Zeitschrift für Naturforschung B55 citationsDOIOpen Access PDF

Abstract

Abstract The presence of Laue oscillations in a film grown on a solid surface is broadly taken as indicating a high quality, crystallographically aligned film of the targeted compound. In this paper we briefly review the origins of both Laue oscillations and Kiessig fringes and show how they can be used together to determine if extra thickness exists above or below the coherently diffracting domains. The differences between experimental and “ideal” films are discussed and the effect of structural features (roughness, different thickness coherently diffracting domains and thickness in addition to the coherently diffracting domains) are illustrated with experimental and simulated data for metal and mixed-metal chalcogenide films of titanium, bismuth, vanadium/iron, and bismuth/molybdenum. Examples are given showing how quantitative information can be extracted from experimental diffraction patterns.

Topics & Concepts

BismuthDiffractionChalcogenideX-ray crystallographyCrystallographyMaterials scienceVanadiumMolybdenumMetalOpticsSurface finishTitaniumSynchrotronSurface roughnessCondensed matter physicsPhysicsChemistryOptoelectronicsMetallurgyComposite materialInorganic Chemistry and MaterialsIron-based superconductors researchSemiconductor materials and interfaces