Litcius/Paper detail

Access to Spirooxindole-Fused Cyclopentanes via a Stereoselective Organocascade Reaction Using Bifunctional Catalysis

Andrea Vopálenská, Vojtěch Dočekal, Simona Petrželová, Ivana Cı́sařová, Ján Veselý

2023The Journal of Organic Chemistry13 citationsDOIOpen Access PDF

Abstract

The present study reports an asymmetric organocascade reaction of oxindole-derived alkenes with 3-bromo-1-nitropropane efficiently catalyzed by the bifunctional catalyst. Spirooxindole-fused cyclopentanes were produced in moderate-to-good isolated yields (15-69%) with excellent stereochemical outcomes. The synthetic utility of the protocol was exemplified on a set of additional transformations of the corresponding spirooxindole compounds.

Topics & Concepts

CyclopentanesBifunctionalOxindoleStereoselectivityChemistryCatalysisOrganocatalysisCombinatorial chemistryReaction conditionsOrganic chemistryEnantioselective synthesisAsymmetric Synthesis and CatalysisOxidative Organic Chemistry ReactionsSynthetic Organic Chemistry Methods