Litcius/Paper detail

Ambiphilic Reactivity of Vinyl Pd-Oxyallyl for Expeditious Construction of Highly Functionalized Cyclooctanoids

Linhong Zuo, Pengchen Ma, Teng Liu, Xiangyang Chen, Robert H. Lavroff, Weipeng Chen, K. N. Houk, Wusheng Guo

2021Organic Letters25 citationsDOI

Abstract

We report the catalytic generation of a vinyl Pd-oxyallyl that dimerizes regiospecifically to form highly functionalized nonbridged cyclooctanoids. Such compounds are otherwise synthetically challenging, but highly useful in synthesis. This vinyl Pd-oxyallyl species demonstrates both electrophilic and nucleophilic properties. DFT calculations elucidate the mechanism and the origins of the chemoselective cyclooctanoid formation.

Topics & Concepts

ChemistryElectrophileReactivity (psychology)NucleophileCatalysisCombinatorial chemistryOrganic chemistryAlternative medicineMedicinePathologyCatalytic Alkyne ReactionsCatalytic C–H Functionalization MethodsCyclopropane Reaction Mechanisms
Ambiphilic Reactivity of Vinyl Pd-Oxyallyl for Expeditious Construction of Highly Functionalized Cyclooctanoids | Litcius