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Synthesis, Characterization, and Optimization of Magnetoelectric BaTiO3–Iron Oxide Core–Shell Nanoparticles

Mahmud Reaz, Ariful Haque, K. Ghosh

2020Nanomaterials34 citationsDOIOpen Access PDF

Abstract

Improvement of magnetic, electronic, optical, and catalytic properties in cutting-edge technologies including drug delivery, energy storage, magnetic transistor, and spintronics requires novel nanomaterials. This article discusses the unique, clean, and homogeneous physiochemical synthesis of BaTiO3/iron oxide core–shell nanoparticles with interfaces between ferroelectric and ferromagnetic materials. High-resolution transmission electron microscopy displayed the distinguished disparity between the core and shell of the synthesized nanoparticles. Elemental mapping and line scan confirmed the formation of the core–shell structure. Energy-dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy detected the surface iron oxide phase as maghemite. Rietveld analysis of the X-ray diffraction data labeled the crystallinity and phase purity. This study provides a promising platform for the desirable property development of the futuristic multifunctional nanodevices.

Topics & Concepts

Materials scienceMaghemiteX-ray photoelectron spectroscopyNanomaterialsNanoparticleNanotechnologyIron oxide nanoparticlesTransmission electron microscopySuperparamagnetismRietveld refinementChemical engineeringMagnetizationCrystallographyChemistryCrystal structureMagnetic fieldEngineeringQuantum mechanicsPhysicsMultiferroics and related materialsMagnetic Properties and Synthesis of FerritesIron oxide chemistry and applications
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