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Nickel-Catalyzed Reductive Cross-Coupling of Aryl Bromides with Vinyl Acetate in Dimethyl Isosorbide as a Sustainable Solvent

Mincong Su, Xia Huang, Chuanhu Lei, Jian Jin

2021Organic Letters23 citationsDOI

Abstract

A nickel-catalyzed reductive cross-coupling has been achieved using (hetero)aryl bromides and vinyl acetate as the coupling partners. This mild, applicable method provides a reliable access to a variety of vinyl arenes, heteroarenes, and benzoheterocycles, which should expand the chemical space of precursors to fine chemicals and polymers. Importantly, a sustainable solvent, dimethyl isosorbide, is used, making this protocol more attractive from the point of view of green chemistry.

Topics & Concepts

IsosorbideChemistryArylNickelVinyl acetateSolventCatalysisOrganic chemistryCoupling (piping)Reductive eliminationCombinatorial chemistryPolymerCopolymerMaterials scienceMetallurgyAlkylCatalytic Cross-Coupling ReactionsCatalytic C–H Functionalization MethodsChemical Synthesis and Reactions
Nickel-Catalyzed Reductive Cross-Coupling of Aryl Bromides with Vinyl Acetate in Dimethyl Isosorbide as a Sustainable Solvent | Litcius