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Determination of the Toxic and Nutrient Element Content of Almonds, Walnuts, Hazelnuts and Pistachios by ICP-AES

Natasa P. Kalogiouri, Natalia Manousi, George A. Zachariadis

2021Separations29 citationsDOIOpen Access PDF

Abstract

The trace element content of thirty-two nuts including almonds, walnuts, hazelnuts and pistachios available in a Greek market was determined by inductively coupled plasma atomic emission spectrometry (ICP-AES). Wet acid digestion using nitric acid (65%) took place in Teflon autoclaves. The limits of detection (LODs) and limits of quantification (LOQs) ranged between 0.01 (Mg)–2.52 (Cu) μg g−1 and 0.02 (Mg)–8.40 (Cu) μg g−1, respectively. Good method linearity (r2 > 0.9990) was observed for each element at the selected emission lines. The metals were quantified and one-way analysis of variance (ANOVA) was used to examine whether or not there were any statistically significant differences among the metal concentrations inside the different nut species.

Topics & Concepts

Inductively coupled plasma atomic emission spectroscopyChemistryNitric acidInductively coupled plasmaAqua regiaFood scienceAnalytical Chemistry (journal)MetalChromatographyInorganic chemistryPlasmaPhysicsQuantum mechanicsOrganic chemistryNuts composition and effectsHeavy Metals in PlantsIsotope Analysis in Ecology