Litcius/Paper detail

Redox-active benzimidazolium sulfonamides as cationic thiolating reagents for reductive cross-coupling of organic halides

Weigang Zhang, Mengjun Huang, Zhenlei Zou, Zheng‐Guang Wu, Shengyang Ni, Lingyu Kong, You‐Xuan Zheng, Yi Wang, Yi Pan

2020Chemical Science38 citationsDOIOpen Access PDF

Abstract

R reagent provides a bench-stable cationic precursor to generate a portfolio of highly active N-S intermediates, which can be successfully applied in cross-electrophilic coupling with various organic halides. The employment of an electrophilic sulfur source solved the problem of catalyst deactivation and avoided odorous thiols, featuring practical conditions, broad substrate scope, and excellent tolerance.

Topics & Concepts

ReagentChemistryHalideCationic polymerizationRedoxCombinatorial chemistryCoupling reactionOrganic chemistryCatalysisSulfur-Based Synthesis TechniquesChemical Synthesis and ReactionsRadical Photochemical Reactions