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Optimizing the mechanical properties of <scp>TiO<sub>2</sub></scp>/<scp>PA12</scp> nano‐composites fabricated by <scp>SLS 3D</scp> printing

Mahmoud Afshari, Soroush Bakhshi, Mohammad Reza Samadi, Hossein Afshari

2022Polymer Engineering and Science23 citationsDOI

Abstract

Abstract In this paper, the selective laser sintering process was used to fabricate the TiO 2 /PA12 nano‐composite parts by considering the parameters of laser power, scanning speed, and TiO 2 content. The response surface methodology was used to improve the mechanical properties of TiO 2 /PA12 nano‐composite parts. The fracture surface characteristics of the specimens were examined using the scanning and transmission electron microscopy. The results indicated that the increase in laser power from 10 to 15 W improved the tensile strength, modulus, and impact strength of the nano‐composite parts because of the fine dispersion of TiO 2 nano‐particles. An increase in the scanning speed from 2000 to 3000 mm/s resulted in the reduction of tensile strength and modulus due to lower heat input and consequently incomplete densification of polyamide‐12. In addition, the increase of TiO 2 content up to 5 wt% can improve the tensile strength, modulus, and impact strength, but requires increasing the laser power. However, the mechanical properties of the nano‐composite parts were enhanced simultaneously at laser power of 12.4 W, scanning speed of 2000 mm/s and TiO 2 content of 1.9 wt%. Moreover, the addition of TiO 2 up to 5 wt% showed a slight influence on thermal stability and crystallinity of the sintered specimens.

Topics & Concepts

Materials scienceUltimate tensile strengthComposite materialScanning electron microscopeSelective laser sinteringComposite numberCrystallinityIzod impact strength testNano-Laser power scalingDispersion (optics)Thermal stabilityLaserSinteringChemical engineeringOpticsEngineeringPhysicsAdditive Manufacturing and 3D Printing TechnologiesAdditive Manufacturing Materials and ProcessesBone Tissue Engineering Materials