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Scanning electrochemical microscopy methods (SECM) and ion-selective microelectrodes for corrosion studies

Ines Traxler, Tanja Denise Singewald, Gabriela Schimo‐Aichhorn, Sabine Hild, Markus Valtiner

2022Corrosion Reviews24 citationsDOIOpen Access PDF

Abstract

Abstract Over the last 30 years, scanning electrochemical microscopy (SECM) has become a fundamental technique in corrosion research. With its high spatial resolution and its ability to study local electrochemistry, it contributes essentially to the understanding of corrosion processes. By using selective micro- and nano-sensors, concentration profiles of different corrosion relevant species, from protons to metal ions, can be established. This review provides a comprehensive overview about SECM based techniques and discusses various types of microsensors, including materials selection and preparation techniques, and it provides extensive tables on redox-couples for specific corrosion research applications.

Topics & Concepts

Scanning electrochemical microscopyCorrosionMaterials scienceMicroelectrodeElectrochemistryNanotechnologyMicroscopyMetallurgyElectrodeOpticsChemistryPhysical chemistryPhysicsElectrochemical Analysis and ApplicationsCorrosion Behavior and InhibitionAnalytical Chemistry and Sensors