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Synthesis of Dioxa-1,7-naphthicorrole and Its Oxidized Porphyrinoid as a Potential Built-In Linker for Biomolecules

Min‐Sung Ko, Jung‐Ho Hong, Adil S. Aslam, Yoon Hee Lee, Dong‐Gyu Cho

2022The Journal of Organic Chemistry11 citationsDOI

Abstract

The first aromatic benzicorrole termed naphthicorrole was synthesized with a carbon donor containing more than six members. Its oxidized (enedione-embedded) porphyrinoid was also obtained using different meso-aryl substitutions under sequential oxidation conditions. The resulting enedione motif of the nonaromatic porphyrinoid was regioselective to the C2 position for S or N nucleophiles. Thus, the oxidized porphyrinoid was tested as a built-in linker for biomolecules. The progress of the reaction was visually monitored due to their different conjugation pathways.

Topics & Concepts

RegioselectivityBiomoleculeLinkerNucleophileChemistryCombinatorial chemistryArylNanotechnologyOrganic chemistryMaterials scienceCatalysisBiochemistryComputer scienceOperating systemAlkylPorphyrin and Phthalocyanine ChemistryPhotosynthetic Processes and MechanismsMetal-Catalyzed Oxygenation Mechanisms
Synthesis of Dioxa-1,7-naphthicorrole and Its Oxidized Porphyrinoid as a Potential Built-In Linker for Biomolecules | Litcius