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Cleavage fracture micromechanisms in thick-section quenched and tempered S690 high-strength steels

Virgínia Bertolo, Quanxin Jiang, Urša Tiringer, Carey L. Walters, Jilt Sietsma, Vera Popovich

2022Journal of Materials Science14 citationsDOIOpen Access PDF

Abstract

Abstract For structural assessment and optimal design of thick-section high-strength steels in applications under harsh service conditions, it is essential to understand the cleavage fracture micromechanisms. In this study, we assess the effects of through-thickness microstructure of an 80-mm-thick quenched and tempered S690 high-strength steel, notch orientation, and crack tip constraint in cleavage nucleation and propagation via sub-sized crack tip opening displacement (CTOD) testing at −100 °C. The notch was placed parallel and perpendicular to the rolling direction, and the crack tip constraint was analysed by varying the a/W ratio: 0.5, 0.25, and 0.1. The notch orientation does not play a role, and the material is considered isotropic in-plane. Nb-rich inclusions were observed to act as the weak microstructural link in the steel, triggering fracture in specimens with the lowest CTOD values. While shallow-cracked specimens from the top section present larger critical CTOD values than deep-cracked ones due to stress relief ahead of the crack tip, the constraint does not have a significant influence in the middle due to the very detrimental microstructure in the presence of Nb-rich inclusions. Some specimens show areas of intergranular fracture due to the combined effect of C, Cr, Mn, Ni, and P segregation along with precipitation of Nb-rich inclusions clusters on the grain boundaries. Several crack deflections at high-angle grain boundaries were observed where the neighbouring sub-structure has different Bain axes.

Topics & Concepts

Materials scienceMicrostructureCrack tip opening displacementCleavage (geology)PerpendicularGrain boundaryComposite materialFracture mechanicsFracture (geology)Crack closureGeometryMathematicsMicrostructure and Mechanical Properties of SteelsFatigue and fracture mechanicsHydrogen embrittlement and corrosion behaviors in metals