Litcius/Paper detail

Enantioselective Intermolecular Heck and Reductive Heck Reactions of Aryl Triflates, Mesylates, and Tosylates Catalyzed by Nickel

Xiaolei Huang, Shenghan Teng, Yonggui Robin, Wenqiang Xu, Maoping Pu, Yun‐Dong Wu, Jianrong Steve Zhou

2020Angewandte Chemie International Edition54 citationsDOIOpen Access PDF

Abstract

Nickel-catalyzed intermolecular Heck reaction of cycloalkenes proceeds well with aryl triflates, mesylates and tosylates in excellent enantiomeric ratios. The asymmetric reductive Heck reaction also works with a 2-cyclopentenone ketal, which is equivalent to conjugate arylation of the enone itself.

Topics & Concepts

NickelArylEnantioselective synthesisHeck reactionIntermolecular forceCatalysisChemistryOrganic chemistryMedicinal chemistryPalladiumMoleculeAlkylCatalytic Cross-Coupling ReactionsCatalytic C–H Functionalization MethodsCyclopropane Reaction Mechanisms