Oil separation from oil in water emulsion by coalescence filtration using kapok fibre
Chandra Jeet Singh, Samrat Mukhopadhyay, R. S. Rengasamy
Abstract
In this study, the stable emulsion of engine oil in water of concentration 10% was prepared using a non-ionic surfactant. Kapok fibres were used as filter beds to separate oil from the oil-water emulsion. The surface morphology of fibres was investigated using Scanning Electron Microscope (SEM) analysis and chemical bond analysis of fibres done using Fourier transform infrared (FTIR). Kapok filter beds were prepared with three different bed heights 10, 20 and 30 mm each with four different porosities 0.90, 0.92, 0.95 and 0.98 for preparing the coalescence filter. The oil-water emulsion (influent) was pumped into the filtration column and the coalesced oil droplets, water, as well as un-coalesced oil droplets, especially the finer oil droplets, were collected as effluent. Oil separation efficiency was evaluated in terms of change in droplet size (D50) and oil concentration from influent to effluent. With increasing porosity and bed height, apart from porosity of 0.92, the separation efficiency increases. Increasing the bed heights at lower porosities does not improve the efficiency of the process. A combination of 0.98 porosity and a bed height of 30 mm provided the highest filtration performance in terms of oil separation efficiency and D50 droplet ratio. At 0.98 porosity, increasing the bed height from 10 mm to 30 mm resulted in a D50 droplet ratio of 0.25-0.14, representing a significant decrease in droplet size in the effluent and therefore an increase in oil separation efficiency from 91.3% to 99.63%.