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Amino-functionalized carbon fiber/polyamide 6 composites with enhanced interfacial and mechanical properties

Yufei Liu, Yikai Zhan, Min He, Chengjun Xiao, Shan Liu, Shuhao Qin, Jie Yu

2022Journal of Materials Research and Technology25 citationsDOIOpen Access PDF

Abstract

Polyamines with different amino numbers were introduced on the surface of carbon fiber (CF) by a chemical grafting method to improve the interfacial properties of CF/polyamide 6 (PA6) composites. First, a carboxyl group was introduced on the surface of CF, and then polyamine was grafted onto the pretreated CF. The chemical structure of CF was confirmed by atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS), polarized light microscopy, and Fourier transform infrared spectroscopy (FTIR), and the performance test results of the composites were systematically analyzed. The content of N on the surface of the modified CF reached 18.92%; the interfacial shear strength (IFSS) and tensile strength of the modified CF/PA6 composite reached 58.6 MPa, respectively, which were 41.5% and 45.5% higher than those of unmodified CF/PA6 composites. The above results confirm that amino-functionalized grafting modification is an effective method to improve the interfacial compatibility and adhesion of composites to improve the mechanical properties of composites.

Topics & Concepts

Materials sciencePolyamideComposite materialX-ray photoelectron spectroscopyFourier transform infrared spectroscopyUltimate tensile strengthGraftingComposite numberSurface modificationPolymerChemical engineeringEngineeringFiber-reinforced polymer compositesbiodegradable polymer synthesis and propertiesTribology and Wear Analysis
Amino-functionalized carbon fiber/polyamide 6 composites with enhanced interfacial and mechanical properties | Litcius