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Catalytic π–π Interactions Triggered Photoinduced Synthesis of Biaryls

Vishal Jyoti Roy, Janardan Chakraborty, Sudipta Raha Roy

2024Organic Letters10 citationsDOI

Abstract

A highly regioselective photocatalytic method to access a variety of biaryl motifs under metal-free conditions has been developed. The organophotocatalyst is involved in π-π stacking interactions with the alkyne species, which promotes this photocatalytic process with thiophene. Mechanistic studies have shed light on these interactions and the overall process. Along with a broad functional-group tolerance and excellent regioselectivity, this protocol has been utilized in the late-stage functionalization of pharmaceuticals and other natural products.

Topics & Concepts

RegioselectivityChemistryStackingCatalysisCombinatorial chemistryPhotocatalysisAlkyneThiopheneSurface modificationFunctional groupPhotochemistryOrganic chemistryPolymerPhysical chemistryCatalytic C–H Functionalization MethodsRadical Photochemical ReactionsSulfur-Based Synthesis Techniques
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