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Discovery and bioinspired total syntheses of unprecedented sesquiterpenoid dimers unveiled bifurcating [4 + 2] cycloaddition and target differentiation of enantiomers

Tao-Bin He, Bing‐Chao Yan, Yuan‐Fei Zhou, Yueqian Sang, Xiao‐Nian Li, Han‐Dong Sun, Chu Wang, Xiao‐Song Xue, Pema‐Tenzin Puno

2023Chemical Science11 citationsDOIOpen Access PDF

Abstract

desymmetrization. The chemical proteomics results showed that a pair of enantiomers shared common targets (PRDX5 C100 and BLMH C73) and had unique targets (USP45 C588 for 4 and COG7 C419 for 9). This work provides experimental evidence for the discovery of unprecedented cadinane dimers from selective Diels-Alder reaction and a powerful strategy to explore the biological properties of natural products.

Topics & Concepts

EnantiomerCycloadditionChemistryStereochemistryOrganic chemistryCatalysisPlant biochemistry and biosynthesisOrganic Chemistry Cycloaddition ReactionsAsymmetric Synthesis and Catalysis
Discovery and bioinspired total syntheses of unprecedented sesquiterpenoid dimers unveiled bifurcating [4 + 2] cycloaddition and target differentiation of enantiomers | Litcius