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Synthesis of Aminated Phenanthridinones via Palladium/Norbornene Catalysis

Xavier Abel‐Snape, Andrew Whyte, Mark Lautens

2020Organic Letters29 citationsDOI

Abstract

-C-H arylation mediated by palladium/norbornene cooperative catalysis is reported. This reaction proceeds through a sequential intermolecular C-N bond formation process followed by intramolecular C-H activation of a tethered arene. The products, aminated phenanthridinones, were generated in moderate to good yields. This method is also applicable to the formation of dibenzazepinones.

Topics & Concepts

ChemistryNorborneneAminationIntramolecular forcePalladiumCatalysisIntermolecular forceCombinatorial chemistryMedicinal chemistryPolymer chemistryOrganic chemistryMoleculePolymerizationPolymerCatalytic C–H Functionalization MethodsSynthesis and Catalytic ReactionsCatalytic Cross-Coupling Reactions
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