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Synthesis and liquid crystalline properties of new triazine-basedπ-conjugated macromolecules with chiral side groups

Nihat Akkurt, Mohammed Hadi Ali Al‐Jumaili, Hale Ocak, Fatih Çakar, Lokman Torun

2020TURKISH JOURNAL OF CHEMISTRY22 citationsDOIOpen Access PDF

Abstract

In this study, we reported the synthesis of a new tribranched macromolecule liquid crystal with triazine in the centre. The central triazine core is bonded via sequences of Sonigashira coupling to 3 triazine unites through acetylenic bridges. The triazines at the periphery are substituted with 2 chiral citronellyloxy side groups. The salt of the resulting star-shaped macromolecule, which was oily at room temperature, with 4-dodecyloxybenzoic acid at 1:1 ratio exhibited a Smectic C (SmC) mesophase. The liquid crystalline properties of organic salt were investigated using DSC (differential scanning calorimetry) and POM (polarizing optical microscopy).

Topics & Concepts

MesophaseMacromoleculeChemistryDifferential scanning calorimetryTriazineSide chainSalt (chemistry)Conjugated systemLiquid crystalPolymer chemistryCrystallographyOrganic chemistryPolymerPhase (matter)Materials scienceOptoelectronicsBiochemistryThermodynamicsPhysicsLuminescence and Fluorescent MaterialsLiquid Crystal Research AdvancementsPhotochromic and Fluorescence Chemistry