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Development of Heterobivalent Theranostic Probes Having High Affinity/Selectivity for the GRPR/PSMA

Rajendra P. Bandari, Terry Carmack, Anil K. Malhotra, Lisa Watkinson, Emily A. Fergason Cantrell, Michael R. Lewis, Charles J. Smith

2021Journal of Medicinal Chemistry24 citationsDOI

Abstract

In this study, we describe the development of heterobivalent [DUPA-6-Ahx-([111In]In-DO3A)-8-Aoc-BBN ANT] and [DUPA-6-Ahx-([177Lu]Lu-DO3A)-8-Aoc-BBN ANT] radiotracers that display very high selectivity/specificity for gastrin-releasing peptide receptor (GRPR)-/prostate-specific membrane antigen (PSMA)-expressing cells. These studies include metallation, purification, characterization, and in vitro and in vivo evaluation of the new small-molecule-/peptide-based radiopharmaceuticals having utility for imaging and potentially therapy. Competitive displacement binding assays using PC-3 cells and LNCaP cell membranes showed high binding affinity for the GRPR or the PSMA. Biodistribution studies showed favorable excretion pharmacokinetics with high tumor uptake in PC-3 or PC-3 prostatic inhibin peptide (PIP) tumor-bearing mice. For example, tumor accumulation at the 1 h time point ranged from (4.74 ± 0.90) to (7.51 ± 2.61)%ID/g. Micro-single-photon emission computed tomography (microSPECT) molecular imaging investigations showed very high uptake in tumors with minimal accumulation of tracers in the surrounding collateral tissues in xenografted mice at 4 h postintravenous injection. In conclusion, [DUPA-6-Ahx-([111In]In-DO3A)-8-Aoc-BBN ANT] and [DUPA-6-Ahx-([177Lu]Lu-DO3A)-8-Aoc-BBN ANT] tracers displayed favorable pharmacokinetic and excretion profiles with high uptake and retention in tumors.

Topics & Concepts

ChemistryLNCaPGlutamate carboxypeptidase IIIn vivoPeptideBiodistributionIn vitroPharmacokineticsCancer researchPharmacologyBiochemistryProstate cancerInternal medicineCancerMedicineBiotechnologyBiologyRadiopharmaceutical Chemistry and ApplicationsPeptidase Inhibition and AnalysisProstate Cancer Treatment and Research
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