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An Exceptionally Stable Metal–Organic Framework Constructed from Chelate-Based Metal–Organic Polyhedra

Jerika A. Chiong, Jie Zhu, Jake Bailey, Mark Kalaj, Rohit H. Subramanian, Wenqian Xu, Seth M. Cohen, F. Akif Tezcan

2020Journal of the American Chemical Society94 citationsDOIOpen Access PDF

Abstract

-tris(hydroxamate) centers, Fe-HAF-1 crystals are negatively charged above pH 4. This unexpected property is attributed to the formation of defects during crystallization that results in uncoordinated hydroxamate ligands or hydroxide-coordinated Fe centers. The anionic nature of Fe-HAF-1 crystals enables selective adsorption of positively charged ions in aqueous solution, resulting in efficient separation of organic dyes and other charged species in a size-selective fashion. Fe-HAF-1 presents a new addition to a small group of chelate-based MOFs and provides a rare framework whose 3D connectivity is exclusively formed by metal-hydroxamate coordination.

Topics & Concepts

ChemistryChelationSupramolecular chemistryAqueous solutionMetalInorganic chemistryAdsorptionCrystallizationHydroxideMetal-organic frameworkMetal hydroxideMetal ions in aqueous solutionPolymer chemistryCrystallographyOrganic chemistryCrystal structureMetal-Organic Frameworks: Synthesis and ApplicationsCrystallography and molecular interactionsX-ray Diffraction in Crystallography
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