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Iron–Phosphine Complex-Catalyzed Intramolecular C(sp<sup>3</sup>)–H Amination of Azides

Siyu Liang, Xiaopeng Zhao, Tonghao Yang, Wei Yu

2020Organic Letters41 citationsDOI

Abstract

Fe(II)–phosphine complex [Fe(dpbz)]Cl2 was demonstrated to be effective for the intramolecular C(sp3)–H amination of organic azides. This catalyst exhibited a high catalytic capacity for the transformations from α-azido amides to imidazolinones. Cyclization of simple aliphatic azides can be realized as well by using [Fe(dpbz)]Cl2 as the catalyst.

Topics & Concepts

ChemistryPhosphineIntramolecular forceAminationCatalysisMedicinal chemistryCombinatorial chemistryOrganic chemistrySynthesis and Catalytic ReactionsCatalytic C–H Functionalization MethodsAsymmetric Hydrogenation and Catalysis
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