Litcius/Paper detail

Large Room Temperature Bulk DNP of <sup>13</sup>C via P1 Centers in Diamond

Daphna Shimon, Kelly A. Cantwell, Linta Joseph, Ethan Q. Williams, Zaili Peng, Susumu Takahashi, Chandrasekhar Ramanathan

2022The Journal of Physical Chemistry C28 citationsDOIOpen Access PDF

Abstract

= ±1) and to blur some of the sharper features associated with the central manifold. The outer lines are best fit using a combination of the cross effect and the truncated cross effect, which is known to mimic features of an Overhauser effect. Similar features are also observed in experiments on single crystal samples. The observation of all of these mechanisms in a single material system under the same experimental conditions is likely due to the significant heterogeneity of the high pressure, high temperature (HPHT) type Ib diamond samples used. Large room temperature DNP enhancements at fields above a few tesla enable spectroscopic studies with better chemical shift resolution under ambient conditions.

Topics & Concepts

SpinsDiamondElectron paramagnetic resonanceMaterials scienceExcitationMicrowaveCrystal (programming language)Analytical Chemistry (journal)Nuclear Overhauser effectElectronNuclear magnetic resonanceMolecular physicsAtomic physicsChemistryNuclear magnetic resonance spectroscopyCondensed matter physicsPhysicsNuclear physicsComputer scienceComposite materialProgramming languageChromatographyQuantum mechanicsAdvanced NMR Techniques and ApplicationsHigh-pressure geophysics and materialsSolid-state spectroscopy and crystallography