Litcius/Paper detail

Lentil protein concentrate + pectin gels dried with SC-CO2: Influence of protein-polysaccharide interactions on the characteristics of aerogels

Srujana Mekala, Marleny D.A. Saldaña

2023The Journal of Supercritical Fluids17 citationsDOIOpen Access PDF

Abstract

This study investigated the interactions of lentil protein concentrate (LPC) and pectin hydrogels and their influence on the physico-chemical characteristics of aerogels. First, emulsion gels were formed using high-intensity ultrasound (HIUS) and the impact of HIUS nominal power, and concentrations of LPC and pectin on the gelation were evaluated. Then, the emulsion gels were dried using supercritical CO 2 (SC-CO 2 ) and the density, surface area, crystallinity index, microstructure and oil and water absorption capacities of the aerogels formed were evaluated. Overall, there was no significant effect of HIUS power on the viscoelastic behavior of the emulsion gels. The emulsion gels exhibited shear-thinning behavior and had thermo-reversible property. The FT-IR spectra of the aerogels showed predominant β-sheets, responsible for the non-covalent bond formation. The aerogels had semi-crystalline structure, densities of 0.0009–0.003 g/mm 3 and surface area of 2.4–7.6 m 2 /g. The LPC-pectin interactions can be explored to form tailor-made aerogels for bioactive delivery.

Topics & Concepts

EmulsionPectinChemical engineeringCrystallinityMaterials scienceSupercritical fluidRheologyViscoelasticityMicrostructureSelf-healing hydrogelsAerogelAbsorption of waterChemistryPolymer chemistryComposite materialOrganic chemistryFood scienceEngineeringProteins in Food SystemsAerogels and thermal insulationFood composition and properties