Litcius/Paper detail

Organic Mixed-Valence Compounds and the Overhauser Effect in Insulating Solids

Svetlana Pylaeva, Patrick Marx, Gurjot Singh, Thomas D. Kühne, Michael Roemelt, Hossam Elgabarty

2021The Journal of Physical Chemistry A22 citationsDOI

Abstract

Recent experiments have shown that the organic free radical 1,3-bisdiphenylene-2-phenylallyl (BDPA) can induce an Overhauser effect dynamic nuclear polarization in insulating solids, a feat previously considered not to be possible. Here, we establish that this peculiar ability of the BDPA radical stems from its mixed-valence nature and the ensuing intramolecular charge transfer. Using state-of-the-art DMRGSCF calculations, we confirm the class II mixed-valence nature of BDPA with the characteristic double-well potential energy surface, and we investigate the mechanism of the consequent electron hopping. A two-component vibronic Hamiltonian is then employed to compute the rate of electron hopping from a quantum dynamical time-propagation of the density matrix. The predicted hyperfine coupling oscillations indeed fall within the frequency range required for an Overhauser effect. The paradigm of mixed-valence compounds as a mining source opens many possibilities for the development and fine tuning of novel polarizing agents.

Topics & Concepts

Valence (chemistry)Intramolecular forceChemistryHamiltonian (control theory)Chemical physicsPolarization (electrochemistry)ElectronPhysical chemistryQuantum mechanicsPhysicsOrganic chemistryMathematicsMathematical optimizationAdvanced Chemical Physics StudiesSolid-state spectroscopy and crystallographyElectron Spin Resonance Studies