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A rapid-quench technique for multi-anvil high-pressure-temperature experiments

Dmitry Bondar, Hongzhan Fei, Anthony C. Withers, Tomoo Katsura

2020Review of Scientific Instruments24 citationsDOI

Abstract

In order to extend the pressure and compositional range where silicate melts can be quenched to form glass in a multi-anvil high-pressure and high-temperature apparatus, a rapid-quench technique, which includes an external cooling system and a low thermal-inertia assembly, was developed. This technique allows much higher cooling rates (6000-7000 °C/s) than regular piston-cylinder (130 °C/s) apparatus and multi-anvil (650 °C/s) apparatus, which are widely used in solid Earth science. Such high cooling rates are critical to avoid unwanted changes in a sample, such as melt crystallization and volatile loss, during quenching.

Topics & Concepts

Materials scienceDiamond anvil cellThermodynamicsHigh pressureMechanicsNuclear engineeringPhysicsEngineeringHigh-pressure geophysics and materialsQuantum, superfluid, helium dynamicsGeological and Geochemical Analysis
A rapid-quench technique for multi-anvil high-pressure-temperature experiments | Litcius