Litcius/Paper detail

A Planar Five‐Membered Aromatic Ring Stabilized by Only Two π‐Electrons

Oleksandr Kysliak, Simon H. F. Schreiner, Niklas Grabicki, Phil Liebing, Florian Weigend, Oliver Dumele∞, Robert Kretschmer

2022Angewandte Chemie International Edition21 citationsDOIOpen Access PDF

Abstract

Abstract Many chemicals known today are partially or fully aromatic, since a ring framework experiences additional stabilization through the delocalization of π‐electrons. While aromatic rings with equal numbers of π‐electrons and ring atoms such as benzene are particularly stable, those with the minimally required two π‐electrons are very rare and yet remain limited to three‐ and four‐membered rings if not stabilized in the coordination sphere of heavy metals. Here we report the facile synthesis of a dipotassium cyclopentagallene, a unique example of a five‐membered aromatic ring stabilized by only two π‐electrons. Single‐crystal X‐ray diffraction revealed a planar Ga 5 ring with almost equal gallium–gallium bond lengths, which together with computational and spectroscopic data confirm its aromatic character. Our results prove that aromatic stabilization goes far beyond what has previously been assumed as minimum π‐electron count in a five‐atom ring fragment.

Topics & Concepts

PlanarRing (chemistry)ElectronMaterials sciencePhysicsAtomic physicsChemistryComputer scienceNuclear physicsComputer graphics (images)Organic chemistrySynthesis and Properties of Aromatic CompoundsSynthesis and characterization of novel inorganic/organometallic compoundsSynthesis and properties of polymers