Synthesis and <sup>83</sup>Kr NMR spectroscopy of Kr@C<sub>60</sub>
Gabriela Hoffman, George R. Bacanu, Elizabeth S. Marsden, Mark C. Walkey, Mohamed Sabba, Sally Bloodworth, Graham J. Tizzard, Malcolm H. Levitt, Richard J. Whitby
Abstract
Synthesis of Kr@C 60 is achieved by a synthetic route that involves quantitative encapsulation of krypton by an open-cage derivative of C 60 . Fine structure is observed in the 13 C NMR spectrum, and 83 Kr NMR characterisation is carried out.
Topics & Concepts
KryptonNuclear magnetic resonance spectroscopyChemistryCarbon-13 NMR satelliteSpectroscopyFluorine-19 NMRAnalytical Chemistry (journal)StereochemistryPhysicsXenonOrganic chemistryQuantum mechanicsFullerene Chemistry and ApplicationsGraphene research and applicationsCarbon Nanotubes in Composites